Argonne national laboratory: 3d printing peek counter-current centrifugal contactor components
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Argonne Nationwide Laboratory: 3D Printing PEEK Counter-Present Centrifugal Contactor Parts

Researchers from Argonne Nationwide Laboratory are analyzing supplies to be used in 3D printing, and have launched ends in the just lately printed ‘Additive Manufacturing Fabrication of PEEK Counter-Present Centrifugal Contactor Parts.’ Whereas the advantages of AM processes are mentioned, there are nonetheless limitations for some forms of manufacturing—regardless of the potential for larger affordability, customization, and on-demand manufacturing.

Relating to fabrication of annular centrifugal contactor-separator levels (CCS), the researchers experimented with high-density acrylic supplies for higher mechanical properties and stronger chemical resistance:

“Over the previous two years, AM has been used to supply low-cost centrifugal contactor elements, starting from bench-scale laboratory testing to a full-scale industrial course of with on-hand availability of spare elements and nice flexibility in design modifications and fast testing and implementation,” acknowledged the researchers.

SLA 3D printing has proved to be inferior for CCS beforehand, with elements failing because of lack of energy in mechanical properties and deterioration of acrylic like flaking, delamination, and extra. Notably, the SLA 3D printed elements may serve effectively as prototypes in analysis and growth, however not for purposeful, industrial use.

MOEX flowsheet utilized for testing of 10 levels of machined PEEK centrifugal
contactors.

Throughout this research, the analysis crew ran seven exams with three extraction, three scrub, and 4 strip levels. Rotors have been scaled up by one centimeter, from 2 cm to three cm. Consequently, TCE evaporation elevated, main the crew to watch and regulate the density of the natural part.

Argonne Nationwide Laboratory: 3D Printing PEEK Counter-Present Centrifugal Contactor Parts

Financial institution of machined PEEK contactors with 10 levels.

“It was found that in ~2 hr of operating the Three-cm financial institution, the density of TBP resolution modified from 1.432 g/mL to 1.419 g/mL,” famous the researchers. “This transformation corresponds to a lack of ~60 mL of TCE per liter of TBP/TCE, and a change in focus of TBP from 30% to 32%. It’s subsequently vital to feed TCE into the natural part reservoir throughout longer runs.”

Because of barely elevated potassium compared to different runs used with AM 2-cm centrifugal contactors, the variety of scrub levels have been elevated, fixing the issue.

Argonne Nationwide Laboratory: 3D Printing PEEK Counter-Present Centrifugal Contactor Parts

The photographs present PEEK filaments following extrusion, (left) earlier than and (proper) after
drying.

The PEEK supplies have been fabricated utilizing FFF 3D printing. Because of intrinsic challenges with each PEEK and FFF 3D printing, the crew relied on an Intamsys FunMat Professional HT, together with virgin PEEK materials and PEEK/Carbon Fiber filament from 3DXTech—added to scale back warping points. The crew additionally took extra measures to take care of moisture, drying the filament for 12 hours.

Argonne Nationwide Laboratory: 3D Printing PEEK Counter-Present Centrifugal Contactor Parts

Semi-crystalline (left) vs amorphous (proper) PEEK

“Hydrodynamic exams together with leak-tightness and zero-point testing demonstrated comparable efficiency between PEEK printed and SLA-printed acrylic CCS levels of the improved design, and dramatically improved efficiency for PEEK printed levels in comparison with the usual rotor design,” concluded the authors. “With the AM fabrication of PEEK contactor levels and the implementation of a fuel purge to guard the motor, all elements are actually both chemically immune to assault by HCl and TCE or are shielded from potential splashing and vapors.”

“Future work will embody finishing up extra holdup testing to raised perceive the composition of phases throughout the mixing part throughout typical operations. A Three-cm contactor housing will have to be printed from PEEK and built-in into an present, historically fabricated Three-cm PEEK CCS financial institution. This integration will additional show the efficiency of PEEK printed contactor levels and can enable for longer-term reliability testing.”

Many alternative analysis initiatives have centered round PEEK, in labs around the globe, from experimenting with recycling isotopes to fabricating disks with antibacterial qualities and optimizing automotive elements. What do you consider this information? Tell us your ideas! Be part of the dialogue of this and different 3D printing subjects at 3DPrintBoard.com.

[Source / Images: ‘Additive Manufacturing Fabrication of PEEK Counter-Current Centrifugal Contactor Components’]

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